Synthesis and X-ray Crystal Structure of a Bridging Trispiran Ligand
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Journal Article
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Publisher
University of Canterbury. Chemistry.
Journal Title
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Date
2004
Authors
Steel, P.J.
Sumby, C.J.
Abstract
Spiro[3,3]heptane-2,6-dispiro-4,5-diazafluorene (4) has been synthesized in three steps from 1,10-phenanthroline. It crystallizes in the orthorhombic space group P2₁2₁2₁ and has the two 4,5-diazafluorene metal binding domains mutually orthogonal.
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Citation
Steel, P.J. and Sumby, C.J. (2004) Synthesis and X-ray Crystal Structure of a Bridging Trispiran Ligand. Arkivoc, 2004(x), pp. 7-12.
Keywords
trispiran, diazafluorene, N-ligand, crystal structure